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The 1st International Seminar on Fundamental and Application ISFAChE 2010 of Chemical Engineering November 3-4, 2010, Bali-Indonesia Table 1: Effect of PEG Concemtration on Yield. Other Operating Variables Kept Constant are: LA=LB=0.5 L/min, [AgNO3]=[KI]=0.05 M, N=4000 rpm Run No. 0402 0401 0924 1018 1020 Concemtration of PEG (M) 0.0 2.5 5.0 10.0 15.0 Yield (%) 100 80 71 78 77 (a) (b) (c) Figure 2: SEM micrographs of prepared AgI atVarious PEG Concentrations. (a) 0.0 g/L, (b) 2.5 g/L, (c) 5.0 g/L, and (d) 15.0 g/L. Operating Variables Kept Constant are: L1=L2=500 mL/min, [AgNO3]=[KI]=0.05 M, N=4000 rpm. Morphology of AgI particles The XRD analysis of AgI particles from run 0401 (in Table 1) presented in Figure 3 showed the characteristic peaks of crystalline silver iodide at (2θ) 22.3, 23.6, 25.3, 39.2, 42.6 and 46.3, which is for β-AgI. Numerous literatures reported that silver iodide usually exists as a mixture of two phases, β-AgI and γ-AgI, below 420K, and the XRD peaks overlap: 23.6, 39.2, and 46.3 for β-AgI and 23.7, 39.1, and 46.3 for γ-AgI [Shaviv et al., 1989 and Wang et al., 2002]. Berry [1967] determined the relative amounts of β-and γ-AgI from measurements of X-ray intensities. Therefore, we probably obtain a mixture of β-AgI and γ-AgI at room temperature. E002-3 (d)PDF Image | Silver Iodide Nanoparticles Using a Spinning Disk Reactor
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