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Crystals 2022, 12, 1290 8 of 9 References efficiency of 99.6% at 2 C under 3.0–4.45 V. This work broadens the application of deep eutectic solvent as a safe electrolyte in high safety and high voltage lithium metal batteries. Author Contributions: W.W. and Q.L. contributed equally to this work. Conceptualization, W.W.; methodology, W.W. and Q.L.; validation, W.W. and Q.L.; formal analysis, W.W. and Q.L.; investigation, W.W. and Q.L.; resources, D.L. and J.L.; data curation, W.W. and M.C.; writing—original draft preparation, W.W. and Q.L.; writing—review and editing, D.L. and J.L.; visualization, W.W. and Q.L.; supervision, M.L. and J.Z.; project administration, M.L. and J.Z.; funding acquisition, J.Z. All authors have read and agreed to the published version of the manuscript. Funding: This work was supported by the National Natural Science Foundation of China (21703218 and U21A20307), Shenzhen Science and Technology Program (JCYJ20180507183907224 and KQTD201708091 10344233), and Guangdong Province COVID-19 Pandemaic Control Research Fund (2020KZDZX1220). Conflicts of Interest: The authors declare no conflict of interest. 1. Lyu, Y.; Wu, X.; Wang, K.; Feng, Z.; Cheng, T.; Liu, Y.; Wang, M.; Chen, R.; Xu, L.; Zhou, J.; et al. An Overview on the Advances of LiCoO2 Cathodes for Lithium-Ion Batteries. Adv. Energy Mater. 2020, 11, 2000982. [CrossRef] 2. Wang, L.; Chen, B.; Ma, J.; Cui, G.; Chen, L. Reviving Lithium Cobalt Oxide-Based Lithium Secondary Batteries-toward a Higher Energy Density. Chem. Soc. Rev. 2018, 47, 6505–6602. [CrossRef] 3. Radin, M.D.; Hy, S.; Sina, M.; Fang, C.; Liu, H.; Vinckeviciute, J.; Zhang, M.; Whittingham, M.S.; Meng, Y.S.; Van der Ven, A. 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Yang, X.; Lin, M.; Zheng, G.; Wu, J.; Wang, X.; Ren, F.; Zhang, W.; Liao, Y.; Zhao, W.; Zhang, Z.; et al. Enabling Stable High-Voltage LiCoO2 Operation by Using Synergetic Interfacial Modification Strategy. Adv. Funct. Mater. 2020, 30, 2004664. [CrossRef] 8. Tuccillo, M.; Palumbo, O.; Pavone, M.; Muñoz-García, A.B.; Paolone, A.; Brutti, S. Analysis of the Phase Stability of LiMO2 Layered Oxides (M = Co, Mn, Ni). Crystals 2020, 10, 526. [CrossRef] 9. Reddy, M.V.; Jie, T.W.; Jafta, C.J.; Ozoemena, K.I.; Mathe, M.K.; Nair, A.S.; Peng, S.S.; Idris, M.S.; Balakrishna, G.; Ezema, F.I.; et al. Studies on Bare and Mg-doped LiCoO2 as a cathode material for Lithium ion Batteries. Electrochim. Acta 2014, 128, 192–197. [CrossRef] 10. Kim, S.; Choi, S.; Lee, K.; Yang, G.J.; Lee, S.S.; Kim, Y. Self-Assembly of Core–Shell Structures Driven by Low Doping Limit of Ti in LiCoO2: First-Principles Thermodynamic and Experimental Investigation. Phys. Chem. Chem. Phys. 2017, 19, 4104–4113. [CrossRef] 11. Yang, Z.; Yang, W.; Tang, Z. Pillared Layered Li1−2xCaxCoO2 Cathode Materials Obtained by Cationic Exchange under Hydrothermal Conditions. J. Power Sources 2008, 184, 557–561. [CrossRef] 12. Caballero, A.; Hernan, L.; Morales, J.; Castellon, E.R.; Santos, J. Enhancing the Electrochemical Properties of Lt-LICoO2 in Lithium Cells by Doping with Mn. J. Power Sources 2004, 128, 286–291. [CrossRef] 13. Zhang, J.-N.; Li, Q.; Ouyang, C.; Yu, X.; Ge, M.; Huang, X.; Hu, E.; Ma, C.; Li, S.; Xiao, R. Trace Doping of Multiple Elements Enables Stable Battery Cycling of LiCoO2 at 4.6 V. Nat. Energy 2019, 4, 594–603. [CrossRef] 14. Liu, L.; Chen, L.; Huang, X.; Yang, X.-Q.; Yoon, W.-S.; Lee, H.; McBreen, J. Electrochemical and in Situ Synchrotron Xrd Studies on Al2O3-Coated LiCoO2 Cathode Material. J. Electrochem. Soc. 2004, 151, A1344. [CrossRef] 15. Tebbe, J.L.; Holder, A.M.; Musgrave, C.B. Mechanisms of LiCoO2 Cathode Degradation by Reaction with Hf and Protection by Thin Oxide Coatings. 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