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TiO2 nano powder and water based nanofluids

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TiO2 nano powder and water based nanofluids ( tio2-nano-powder-and-water-based-nanofluids )

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Kavitha T et al Euro. J. Appl. Eng. Sci. Res., 2012, 1 (4):235-240 ______________________________________________________________________________ Table1: Thermal conductivity of various solids and liquids Carbon Metallic solids (pure) Nonmetallic solids Metallic liquids Nonmetallic liquids Material Nanotubes Diamond Graphite Fullerenes film Copper Aluminum Silicon Alumina (Al2O3) Sodium (644 K) Water Ethylene glycol (EG) Engine oil (EO) Thermal conductivity (W/mK) 1800-6600 2300 110-190 0.4 401 237 148 40 72.3 0.613 0.253 0.145 MATERIALS AND METHODS 2. Experimental Study 2.1 Synthesis and preparation methods The Preparation of nanofluids is the first key step in experimental studies with nanofluids. 2.1.1 Two step technique Two-step method is the most widely used method for preparing nanofluids. Nanoparticles, nanofibers, nanotubes, and nanomaterials. In this method, first produced as dry powders by using chemical or physical methods [6-9]. We used sol gel technique for preparation of nano Tio2 powders [8]. The obtained nanosized powder will be dispersed into a base fluid (Water) in the second processing step with the help of intensive magnetic force agitation. 2.1.2 Nano Tio2 preparation by using sol gel technique TiO2 Nano-powders were prepared via sol–gel method using titanium tetraisopropoxide (TTIP, Merck), distilled water, ethyl alcohol (EtOH, Merck) as the starting materials. Titanium tetraisopropoxide was dropped slowly into the solution of water and ethyl alcohol while magnetic agitating continuously to get white slurry solution [36]. The obtained solutions were kept under slow-speed constant stirring on a magnetic stirrer for 40mins at room temperature [12]. Then the precipitated TiO2 was filtered and dried at 50oC for 1 h until it was turned into white block crystal. After ball milling the dried powders obtained were calcinated at 400oC for 2 h to observe the phase changes accompanying the heat treatments [10-12]. 2.2 Nanofluids preparation using Tio2 nanoparticles The TiO2 Nano particles have an average size of 6 nm used for investigation in the present experimental work. The photographic view of the nanoparticles as seen by the naked eyes is shown in the Figure 2.1 [12, 13]. The distribution of TiO2 nanoparticles at Nano scale can be observed under a Scanning Electron Microscope (SEM). The SEM images of TiO2 nanoparticles as shown in the figure 3.2 [35-37]. Preparation of nanofluids is an important stage and nanofluids are prepared in a systematic and careful manner [13-16]. A stable nanofluid with uniform particle dispersion is required and the same is used for measuring the thermo physical properties of nanofluids [17]. Figure 2.1: Photographic view of Tio2 nanoparticles Scholars Research Library 236

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