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Experimental section The samples used for the present study were new commercial low-silica zeolites, LiLSX and NaLSX (Tricat GmbH, Bitterfeld, Germany), own synthesis products of AlPO4-5, AlPO4-17, AlPO4-18 and SAPO-34 as well as the with CaCl2 impregnated silica gel, attapulgite and activated carbon, respectively, with different pore size distributions. The SAPO for the measurements on the kg-scale was a specially designed pelleted product for this purpose. The micro-, meso- and macroporous materials (microporous active carbon, two types of silica gel with mesopores (1) and macropores (2) and attapulgite with small macropores or big mesopores) were impregnated (in all cases) with 30% CaCl2. The salt was mainly accommodated in the pores. For the TG- experiments a LiNaX zeolite was used which was obtained by a Li-ion exchange of the Na-form of a commercial available X-zeolite (from CWK, Bad KoĢstritz, Germany). Figure 1 Scheme of the 1.5 L thermochemical storage unit for 1 kg material. Figure 2 Picture of the 1.5 L thermochemical storage unit for 1 kg material, the arrangement of the unit parts corresponds with the scheme in Figure 1. 7th Workshop of IEA/ECES Annex 17, 8-12 October 2004, Beijing, PR of China 2PDF Image | STORAGE OF LOW TEMPERATURE HEAT BY ZEOLITES
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