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Chapter 6 β Production of Few Layer Graphene in Aqueous Media for Biological Studies Figure 6.6: a), d), g) and j) representative AFM height scans, b), e), h) and k) histograms of length of graphene flake (πΏπ΄πΉπ), c), f), i) and l) histogram of number of layers per flake (π) of starting G/DMF, starting G/NMP, 0.1 v/v% dialysed G/DMF and 0.1 v/v% dialysed G/NMP, respectively. The presence of a large number of relatively thin and smaller-sized graphene flakes (range of 50-100 nm) was observed (Figure 6.6j and Appendix 9.3). Some of the smaller flakes had no defined edges, compared to the other graphene flakes. This observation, as reported recently382, could be due to the crumpling of thin pristine graphene sheets (from aqueous media) as a result of the AFM spray preparation process.382 171PDF Image | PRODUCTION AND APPLICATIONS OF GRAPHENE AND ITS COMPOSITES
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