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27 soaked in 0.5 M sulfuric acid at the same temperature for another hour, followed again by 28 rinsing with DI water. Lastly, they were soaked in DI water at 100◦C for one more hour and 29 then stored in DI water prior to use. The frit was glued into its acrylic frame using Devcon 30 2 Ton Epoxy from McMaster-Carr before assembly. 31 During assembly, the membranes were trimmed to the appropriate size using a razor 32 blade. The gasketing material was used to seal the device and house the electrode channels 33 that had been cut into the gaskets. The electrode channels were open and pressurized during 34 operation using downstream pressure tubing in order to hold the membranes flat against the 35 frit. The splitter was also made from teflon gasketing material that was compressed against 36 the end of the frit using the outlet port plate. The device was assembled using five 1.5 in. 37 8-32 and four 2 in. 6-32 316 stainless steel bolts (McMaster-Carr) that were wrapped with 38 electrical tape to minimize corrosion. The 8-32 bolts were tightened to 25 in-lbs of torque 39 and the 6-32 bolts were tightened during operation until no more leaks were observed. 40 Additional Figures 41 Please note that the errorbars in all figures for ion removal, concentration, and energy/current 42 efficiency represent one standard deviation (for 4-8 realizations) about the mean and that 43 the errorbars in all figures for water recovery represent a combination of the range about the 44 mean and an estimate for maximum bias due to the measurement method. S3PDF Image | Continuous Water Deionization by Shock Electrodialysis
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