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Material synthesis and characterization Column chromatography with silica gel from VWR Scientific was used for flash chromatography. Microwave experiments were carried out in a Biotage Initiator V 2.3. 1H and 13C NMR spectra were recorded on a Bruker AV-400 spectrometer at 298 K and are reported in ppm relative to TMS. UV-Vis absorption spectra were recorded on UV-1601 (λmax 1100 nm) UV-VIS Shimadzu spectrometers. MALDI TOF spectrometry was carried out in positive reflection mode on a Micromass MALDImxTOF with trans-2-[3-(4-tert-Butylphenyl)-2-methyl-2-propenylidene]-malononitrile (DCTB) as the matrix. Cyclic voltammograms were recorded on an Autolab PGSTAT101 with a standard three-electrode setup with ITO coated glass slides, a Pt counter electrode and a Ag/AgCl reference electrode (calibrated against ferrocene (Fc/Fc+)). The measurements were either carried in an anhydrous, degassed 0.1 M tetrabutylammonium hexafluorophosphate (TBAPF6) acetonitrile solution or in a 0.1 M NaCl aqueous solution as the supporting electrolyte with a scan rate of 100 mV/s. Gel permeation chromatography (GPC) measurements were performed on an Agilent 1260 infinity system operating in DMF with 5 mM NH4BF4 with 2 PLgel 5 μm mixed-C columns (300×7.5mm), a PLgel 5 mm guard column (50x7.5mm) at 50 °C with a refractive index detector as well as a variable wavelength detector. The instrument was calibrated with linear narrow poly(methyl methacrylate) standards in the range of 0.6 to 47kDa. Dialysis was carried out in a dialysis kit Thermo Scientific Slide-A-Lyzer Cassette with a molecular weight cut off of 2K. The deionised water was replaced every 6 h and the dialysis was carried out for two days. End-capping procedure: After the reaction was cooled to room temperature, 0.1 mL of a solution made of 1.00 mg of Pd2(dba)3 and 0.1 mL of 2-(Tributylstannyl)thiophene in 0.5 mL of anhydrous degassed DMF was added and heated for 1 h to 100 °C, then 0.1 mL of a solution made of 1.00 mg of Pd2(dba)3 and 0.1 mL of 2-bromothiophene in 0.5 mL of anhydrous degassed DMF was added and heated to 100 °C. 17PDF Image | salt water battery with high stability
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Product and Development Focus for Infinity Turbine
ORC Waste Heat Turbine and ORC System Build Plans: All turbine plans are $10,000 each. This allows you to build a system and then consider licensing for production after you have completed and tested a unit.Redox Flow Battery Technology: With the advent of the new USA tax credits for producing and selling batteries ($35/kW) we are focussing on a simple flow battery using shipping containers as the modular electrolyte storage units with tax credits up to $140,000 per system. Our main focus is on the salt battery. This battery can be used for both thermal and electrical storage applications. We call it the Cogeneration Battery or Cogen Battery. One project is converting salt (brine) based water conditioners to simultaneously produce power. In addition, there are many opportunities to extract Lithium from brine (salt lakes, groundwater, and producer water).Salt water or brine are huge sources for lithium. Most of the worlds lithium is acquired from a brine source. It's even in seawater in a low concentration. Brine is also a byproduct of huge powerplants, which can now use that as an electrolyte and a huge flow battery (which allows storage at the source).We welcome any business and equipment inquiries, as well as licensing our turbines for manufacturing.CONTACT TEL: 608-238-6001 Email: greg@infinityturbine.com (Standard Web Page)