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PREPARATION OF LIGHT STABLE HOP PRODUCTS

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PREPARATION OF LIGHT STABLE HOP PRODUCTS ( preparation-light-stable-hop-products )

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15 separatingthemixtureofthehop solidsandthe?rstalcohol solvent into treated hop solids and a ?rst ?ltrate includ ingalpha/iso-alphaacids; mixing the treated hop solids With a second alcohol solvent toformamixtureofthetreatedhop solidsandthesecond alcoholsolvent; separating the mixture of the treated hop solids and the second alcohol solvent into hop solids residues and a second?ltrateincludingalpha/iso-alphaacids,Wherein 10 a light stable hop product comprising the hop solids residuesisformed, mixingatleastoneofthe?rst?ltrateandthesecond?ltrate With a metal ion that complexes With alpha/iso-alpha acids to form a mixture including metal ion-alpha/iso alphaacidscomplexes; separatingthemetalion-alpha/iso-alphaacidscomplexes from the mixture including metal ion-alpha/iso-alpha acids complexes to form a third ?ltrate; and mixing the hop solids residues With the third ?ltrate such thatthelightstablehopproductcomprisesthehopsolids residues and the third ?ltrate. 16 22. The method ofclaim 21 Wherein: the step of mixing at least one of the ?rst ?ltrate and the second ?ltrate With the metal ion comprises mixing at least one of the ?rst ?ltrate and the second ?ltrate With a compound selected from the group consisting of cal cium carbonate, calcium hydroxide, magnesium hydroxide,magnesiumcarbonate,magnesiumacetate, Zincsulfate,andZincacetate, such that metal ion-alpha/iso-alpha acids complexes pre cipitate out of at least one of the ?rst ?ltrate and the second ?ltrate. 23. The method of claim 21 further comprising: concentrating the hop solids residues and the third ?ltrate aftermixingsuchthatthelightstablehopproductcom prises a concentrated mixture of the hop solids residues andthethird?ltrate. 24. The method of claim 21 further comprising: mixing the hop solids residues With an additive selected fromthegroupconsistingofhopoilfractions,beta-acid richfractions,lightstablebitteringagentsandmixtures thereofsuchthatthelightstablehopproductcomprises thehopsolidsresidues,thethird?ltrate,andtheadditive. * * * * * US 7,413,758B2 5

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PREPARATION OF LIGHT STABLE HOP PRODUCTS

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