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44 45 46 47 48 down down down down r482 568 620 689 80 ' 744 , Pressure (bar) 207 TABLE I Solubility (wt. %)“ cottonseed down soybean down soybean down soybean down soybean down soybean down soybean down 55' 964 60 207 60 344 1839 60 482 919 60 551 919 60 620 919 60 689 460 cottonseed cottonseed cottonseed cottonseed 22.56 4.90. up 60 758 681 36.71 5.39 up 60 827 681 45.62 6.70 up 60 895 454 34.46 7.59 29 30 31 1 cottonseed up 32 soybean down 33 soybean down 34 soybean down 35 soybean down 36 I soybean down 37 soybean down 70 689 -38 'cottonseed down 39 cottonseed up 40 cottonseed down 70 758 ' 41 ‘cottonseed 42 cottonseed 43 drymilled down ' corn germ cottonseed cottonseed I cottonseed cottonseed down 80 268 1067 2.74 0.26 I_ up 60 60 70 _ 70 344 70 482 70 5'51 70 620 681 68.48 10.06 5 4,466,923 TABLE I Direction Flaked ofsolvent Temperature Pressure throughsubstrate collected Solubility CO2 passed Oil Example substrate ?ow ('C.) (bar) (g.) '' (g) (%) 1 2 3 4 ’5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 soybean soybean soybean soybean soybean cottonseed cottonseed down 40 1033 1362 40.11 2.94 down 40 207 431 1.9 0.44 down 40 344 2758 25.63 0.93 down 40 482 919 15.36 1.67 down 40 551 1107 ' 21.59 1.95 down 40 620 910 20.08 2.21 down 40 758 454 11.71 2.58 soybean down 50 soybean down 50 soybean down 50 soybean down 50 soybean down 50 soybean down so cottonseed down 50 758 959 36.69 3.83 50 895 50 964 50 _1033 55 665 454 ' 21.87 4.82 207 2724 9.06 0.33 344 482 551 454 12.25 2.70 620 908 ‘ 28.38 3.13 689 1561 54.17 3.47 ' cottonseed up cottonseed up cottonseed up cottonseed down cottonseed down 55 827 454 23.27 5.13 964 1033 207 454 2298 919 64.3 14.16 1.25 0.05 8.7 0.95 409 26.62 - 454 36.68 70 802 v 233 > 72.12 70 ' 812 227 31.23 70 v 827 227 v 46.98 up 70 854 ' 113 48.92 6.51 8.08 30.95" 13.76 v 20.70 43.29“ 13.84 3.05 . ' 46.95 5.17 59.99 6.61 ' 119.18 8.75 130.96 14.42 40° C. 50° C. 55° C. 60° C. 70° C. 80° C. (Ex.l-7) (Ex.8-17) (Ex.18-20) (EX.21-31) (Ex.32-42) (Ex.43-48) > 80 i. \ 80 _ 801 ' 80 ‘ 454 908 908 v '1362 908 cottonseed down “Thesevaluesrepresenttheweightrelationshipbetweenextractedoiland CO2 solvent,butnotnecessarilytheactualsolubility. 0.44 0.33 — 0.1 l 0.05 —— 268——————0.26 344 0.93 1.21 — 1.12 0.95 — 482 .1.67 2.35 — 2.54 2.77 3.05 1816 21.91 _ 1.21 1362 32.03 2.35 4.61 454 26.42 5.82 6041 6.78 0.11 20.6 1.12 23.37 2.54 30.45 3.31 36.08 3.93 908 681 908 41.86 1 32.2 35.69 4.73 ' 3.93 919 25.43 2.77 919 35.74 3.89 1379 73.34 v ' 5.32PDF Image | SUPERCRITICAL CO2 EXTRACTION OF LIPIDS
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