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HO O Cl O O (step 4) O O O O O Figure A.14 14-crown-4 monomer synthesis step 4 In the fifth step, the product was mixed with mesyl chloride (See Figure A.15). Mesyl chloride was put into a reaction balloon which was placed in an ice bath and the product of step 4 was dripped onto it. After dripping, the mixture was taken into room temperature and mixed for 60 hours. O O SCl O O Figure A.15 14-crown-4 monomer synthesis step 5 In the sixth step, the product after step 5 was mixed with the product which was acquired after step 3 and a condensation reaction was expected to synthesize a crown-4-ether structure (See Figure A.16). While dripping, a phase separation occurred in the mixture. The reaction was continued for 15 hours at 80 oC. The hexane phase was separated into another erlenmeyer and put aside. The remaining black residue was held in the balloon. OO Li+ OO O ClOOOLiLiO O Figure A.16 14-crown-4 monomer synthesis step 6 O O S OO Afterwards a TLC experiment was done in order to understand how many products were in the hexane phase. TLC paper showed, 7 separate dots, which designates 7 163 O S O Cl O (step 5) O (step6)PDF Image | SEPARATION OF LITHIUM FROM BRINES
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Product and Development Focus for Infinity Turbine
ORC Waste Heat Turbine and ORC System Build Plans: All turbine plans are $10,000 each. This allows you to build a system and then consider licensing for production after you have completed and tested a unit.Redox Flow Battery Technology: With the advent of the new USA tax credits for producing and selling batteries ($35/kW) we are focussing on a simple flow battery using shipping containers as the modular electrolyte storage units with tax credits up to $140,000 per system. Our main focus is on the salt battery. This battery can be used for both thermal and electrical storage applications. We call it the Cogeneration Battery or Cogen Battery. One project is converting salt (brine) based water conditioners to simultaneously produce power. In addition, there are many opportunities to extract Lithium from brine (salt lakes, groundwater, and producer water).Salt water or brine are huge sources for lithium. Most of the worlds lithium is acquired from a brine source. It's even in seawater in a low concentration. Brine is also a byproduct of huge powerplants, which can now use that as an electrolyte and a huge flow battery (which allows storage at the source).We welcome any business and equipment inquiries, as well as licensing our turbines for manufacturing.| CONTACT TEL: 608-238-6001 Email: greg@infinityturbine.com | RSS | AMP |