PDF Publication Title:
Text from PDF Page: 186
+Na-O OH Br Figure A.12 14-crown-4 monomer synthesis step 2 Br 24h 70-80 oC OO OH HO (step 2) In third step, the product was mixed with butyl lithium in a molar ratio of 1:2 (See Figure A.13). Butyl lithium could be stored in hexane solution, therefore the reaction continued in hexane medium at room temperature for 8 hours. OO OH HO 2 Li OO OLi LiO (step 3) Figure A.13 14-crown-4 monomer synthesis step 3 In the fourth step, glycidol was dissolved with equivolume dichloromethane (See Figure A.14). Then, benzoyl chloride was dissolved with equivolume dichloromethane and pyrridine was dissolved with equivolume dichloromethane. Equimolar benzoyl chloride and pyrridine solutions were dripped onto equimolar glycidol solution simultaneously. The reaction was held on in an ice bath under vigorous stirring for 15 hours. After the reaction was completed, the product mixture was taken into separation funnel. Ice-water and sodium chloride was added to funnel and the funnel was shaken vigorously. Then the phase separation was observed in the funnel. The dichloromethane phase was taken and mixed with sodium sulfate in order to separate remaining water residues. In the rotary evaporator, the dichloromethane was evaporated and an orange colored viscous liquid was taken as a product. 162PDF Image | SEPARATION OF LITHIUM FROM BRINES
PDF Search Title:
SEPARATION OF LITHIUM FROM BRINESOriginal File Name Searched:
separation-lithium-from-brine.pdfDIY PDF Search: Google It | Yahoo | Bing
Product and Development Focus for Infinity Turbine
ORC Waste Heat Turbine and ORC System Build Plans: All turbine plans are $10,000 each. This allows you to build a system and then consider licensing for production after you have completed and tested a unit.Redox Flow Battery Technology: With the advent of the new USA tax credits for producing and selling batteries ($35/kW) we are focussing on a simple flow battery using shipping containers as the modular electrolyte storage units with tax credits up to $140,000 per system. Our main focus is on the salt battery. This battery can be used for both thermal and electrical storage applications. We call it the Cogeneration Battery or Cogen Battery. One project is converting salt (brine) based water conditioners to simultaneously produce power. In addition, there are many opportunities to extract Lithium from brine (salt lakes, groundwater, and producer water).Salt water or brine are huge sources for lithium. Most of the worlds lithium is acquired from a brine source. It's even in seawater in a low concentration. Brine is also a byproduct of huge powerplants, which can now use that as an electrolyte and a huge flow battery (which allows storage at the source).We welcome any business and equipment inquiries, as well as licensing our turbines for manufacturing.CONTACT TEL: 608-238-6001 Email: greg@infinityturbine.com (Standard Web Page)