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1) Sequence I – Uniform Maximum strain A total of four to five deformation cycles (loading and unloading) with a maximum strain level of 0.3 % strain. 2) Sequence II – Increased Maximum strain A total of five deformation cycles with 0.1 %, 0.2 %, 0.3 %, 0.4 % and 0.5 % strain as the maximum strain at each cycle. 3) Sequence III – Strain Mapping To demonstrate the longer term stability and spatial mapping, a total of 25 cycles with a maximum strain of 0.3 % was employed. 5 random points were studied at the maximum and minimum of each cycle. Detailed spatial maps were taken on initial, 6th and 25th cycles at step intervals of 10 ± 2 μm. 4) Sequence IV – Variable Maximum strain A total of nine deformation cycles with maximum strain of 0.3 % strain for first 3 cycles, 0.5 % for subsequent three cycles and 0.3 % for last three cycles. It has to be noted that the sequence I and II were carried out for both mechanically exfoliated and CVD graphene coatings. Whereas, sequence IV was subjected only for mechanically exfoliated graphene coating to explore about the strain hardening behaviour, and sequence III was carried out only for CVD graphene coating to study the wide-area strain sensing behaviour. Chapter 4 – Methods 129PDF Image | PRODUCTION AND APPLICATIONS OF GRAPHENE AND ITS COMPOSITES
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