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Table of Contents 1. Introduction .................................................................................................................................. 9 2. Publications and patents.............................................................................................................11 3. Graphene-based materials..........................................................................................................12 4. Existing production routes .........................................................................................................13 5. Liquid-phase exfoliation ............................................................................................................ 15 5.1 Precursor ............................................................................................................................ 15 5.2 Graphene dispersion...........................................................................................................19 5.2.1 Solvents ...................................................................................................................... 19 5.2.2 Surfactants.................................................................................................................. 23 5.2.3 Reductive dissolution .................................................................................................26 5.3 Exfoliation mechanisms.....................................................................................................27 5.3.1 Mechanical exfoliation ............................................................................................... 28 5.3.2 Chemical exfoliation .................................................................................................. 28 5.3.3 Electrochemical exfoliation ....................................................................................... 31 5.4 Exfoliation methods ........................................................................................................... 31 5.4.1 Solvothermal route ..................................................................................................... 32 5.4.2 Microwave irradiation ................................................................................................ 34 5.4.3 Supercritical Fluids ....................................................................................................37 5.4.4 Vortex fluidic device..................................................................................................38 5.4.5 Taylor-Couette device ................................................................................................ 40 2PDF Image | graphene production via nonoxidizing liquid exfoliation
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