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to ‘separate’ the contribution of both electrodes to this MF loop, and symmetric coin cells were prepared and characterized. 6.3.1. Symmetric coin cells approach Figure 6-2 shows Nyquist plots of symmetric cells composed of two similar electrodes (Li||Li, S8||S8), which are compared with a complete Li/S cell. (a) (b) (c) Chapter 6: EIS and low temperature studies Figure 6-2. Nyquist plot obtained for Li/S complete cell (in black), symmetric Li||Li (in red) and S8||S8 (in blue) (a,b); zoomed image on the S8||S8 semicircle (c). To confirm the validity of the symmetric cell approach, experimental data of the complete cell (Li/S) were compared with the calculated one (Figure 6-3), according to equation: ZLi-S = 1⁄2 ZLi-Li + 1⁄2 ZS-S. Both graphs are superimposed in the whole frequency range, proving the validity of the symmetric cell approach used for separation of both electrodes to the spectrum of the complete cell. 194PDF Image | Accumulateur Lithium Soufre
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