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Chapter 5: In situ and operando XRD Figure 5-12. Evolution of S8 consumption and Li2S formation upon discharge, and determination of correlation between practical discharge capacity and peaks areas of in situ XRD patterns. To this purpose, Figure 5-12 allows to correlate the real and experimentally obtained evolution of S8 and Li2S peaks areas as compared to the practical capacity (in mAh g-1). Thus, in the first part of Li2S formation (1st step), the ratio between sulfur disappearance and Li2S appearance experimentally obtained is 0.75, calculated as follow: 06-7& -A 01 #77&#$# !& = 2.05 = 0.75 =PDF Image | Accumulateur Lithium Soufre
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